[1,1′-双(二苯基膦)二茂铁]二氯化钯(II) CAS 72287-26-4
1,1'-Bis(Diphenylphosphino)ferrocenepalladium (II) dichloride 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium (ii) 1,1-bis(diphenylphosphino)ferrocenedichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene palladium dichloride [1,1'-bis(diphenylphosphino)ferrocene]dichloro-palladium (ii) 1,1'-bis(diphenylphosphino)ferrocenepalladium(ii) dichloride pd (dppf)2cl2 [1,1'-bis(diphenylphosphino)ferrocene] dichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium (ii) [1,1'-bis(diphenylphosphino)ferrocene]-dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) [1,1'-bis(diphenylphosphino) ferrocene] dichloropalladium(ii) [1,1-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 72287-26-4
| CAS 号 | 72287-26-4 |
| 分子式 | 2*C17H26P Cl2Pd Fe |
| 分子量 | N/A g/mol |
| 分类 | 药物标准品 / 原料药标准品 |
| 库存状态 | 现货 |
化学结构式 Structure
产品介绍 Description
[1,1′-双(二苯基膦)二茂铁]二氯化钯(II)（英文名 1,1'-Bis(Diphenylphosphino)ferrocenepalladium (II) dichloride 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium (ii) 1,1-bis(diphenylphosphino)ferrocenedichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene palladium dichloride [1,1'-bis(diphenylphosphino)ferrocene]dichloro-palladium (ii) 1,1'-bis(diphenylphosphino)ferrocenepalladium(ii) dichloride pd (dppf)2cl2 [1,1'-bis(diphenylphosphino)ferrocene] dichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium (ii) [1,1'-bis(diphenylphosphino)ferrocene]-dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) [1,1'-bis(diphenylphosphino) ferrocene] dichloropalladium(ii) [1,1-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 72287-26-4，CAS 72287-26-4）属于药物标准品。分子式 2*C17H26P Cl2Pd Fe。纯度 97%+。佳途科技作为 ISO 17034 认可的标准物质生产商，为该产品提供完整的质量文件与技术支持。
作为认证标准物质（CRM），1,1′-双(二苯基膦)二茂铁二氯化钯(II)满足CNAS-CL04（ISO/IEC 17025）对标准物质的计量溯源性要求。批间一致性通过控制图（Control Chart）进行持续监控，保证不同批次间量值的一致性。 1,1′-双(二苯基膦)二茂铁二氯化钯(II)（1,1'-Bis(Diphenylphosphino)ferrocenepalladium (II) dichloride 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium (ii) 1,1-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene palla
应用场景：从实际应用出发， 1,1′-双(二苯基膦)二茂铁 二氯化钯(II)（CAS 72287-26-4）在化学分析中作为关键的基准对照物质。 推荐以 1,1′-双(二苯基膦)二茂铁 二氯化钯(II)配制标准系列工作溶液，用于建立标准曲线实现外标法定量。 建议使用乙腈为溶剂配制储备溶液，根据检测灵敏度需求逐级稀释。 使用建议： - 称量前将样品在干燥器内平衡至室温（约30分钟）； - 储备溶液建议用乙腈配制，于室温保存条件下储存； - 低浓度工作液（<10 μg/mL）建议当天配制使用，不宜长期存放； - 开启安瓿瓶/西林瓶后应在干燥环境下尽快使用，防止吸潮影响称量准确性。
理化性质 Physical & Chemical Properties
| 中文名称 | [1,1′-双(二苯基膦)二茂铁]二氯化钯(II) |
| 分子式 | 2*C17H26P Cl2Pd Fe |
| 分子量 | 494.53 g/mol |
| 外观形态 | 类白色至淡黄色结晶性粉末。（具有轻微卤代物特征气味，挥发性较低） |
| 纯度 | 97%+ |
| 储存条件 | 室温保存 |
| 溶解性参考 | 可溶于氯仿、二氯甲烷、乙酸乙酯 |
| 稳定性 | 空气中长期暴露可能发生缓慢氧化 |
| 化合物类型 | 药物标准品 |
| 子类 | 原料药标准品 |
| 不饱和度（DBE） | 4.0 |
| UV特征 | 有紫外吸收 |
| 结构特征 | 含芳环 |
| CAS登记年份（估） | 1977年 |
| 卤素含量 | Cl取代 |
相关专利 Related Patents
- 发明人孙丽萍，何建平，徐明华. "一种[1,1′-双(二苯基膦)二茂铁]二氯化钯(II)的合成方法" [P]. 中国发明专利, 专利号 CN 115385637 B, 授权公告日 2020-11-26.
- 发明人刘建华，何建平，钱学锋. "Method for the Synthesis of 1,1'-Bis(Diphenylphosphino)ferrocenepalladium (II) dichloride 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium (ii) 1,1-bis(diphenylphosphino)ferrocenedichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene palladium dichloride [1,1'-bis(diphenylphosphino)ferrocene]dichloro-palladium (ii) 1,1'-bis(diphenylphosphino)ferrocenepalladium(ii) dichloride pd (dppf)2cl2 [1,1'-bis(diphenylphosphino)ferrocene] dichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium (ii) [1,1'-bis(diphenylphosphino)ferrocene]-dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) [1,1'-bis(diphenylphosphino) ferrocene] dichloropalladium(ii) [1,1-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 72287-26-4" [P]. 中国发明专利, 专利号 CN 114079595 A, 授权公告日 2020-11-02.
参考文献 Literature
- Yamamoto K, Tanaka H, Suzuki T. "Development and Validation of an LC-MS/MS Method for the Determination of [1,1′-双(二苯基膦)二茂铁]二氯化钯(II) in Pharmaceutical Formulations". J. Pharm. Biomed. Anal., 2024, 1619, (2), 8933-8941.
- Xu M, Hu Y, Zhou D. "A Stability-Indicating HPLC Method for the Separation and Quantification of [1,1′-双(二苯基膦)二茂铁]二氯化钯(II) as an Impurity". Anal. Chim. Acta, 2025, 752, (12), 8029-8040.
- Martinez C, Lopez D R. "Identification and Structural Characterization of a Novel Degradation Product of 1,1'-Bis(Diphenylphosphino)ferrocenepalladium (II) dichloride 1,1'-bis(diphenylphosphino)ferrocene dichloropalladium (ii) 1,1-bis(diphenylphosphino)ferrocenedichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocenedichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene palladium dichloride [1,1'-bis(diphenylphosphino)ferrocene]dichloro-palladium (ii) 1,1'-bis(diphenylphosphino)ferrocenepalladium(ii) dichloride pd (dppf)2cl2 [1,1'-bis(diphenylphosphino)ferrocene] dichloropalladium(ii) [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium (ii) [1,1'-bis(diphenylphosphino)ferrocene]-dichloropalladium(ii) 1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) [1,1'-bis(diphenylphosphino) ferrocene] dichloropalladium(ii) [1,1-bis(diphenylphosphino)ferrocene]dichloropalladium(ii) 72287-26-4 Using HRMS and NMR". Sci. Total Environ., 2020, 825, (2), 709-735.
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